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Description of ASTM-D7550 2009ASTM D7550 - 09Standard Test Method for Determination of Ammonium, Alkali and Alkaline Earth Metals in Hydrogen and Other Cell Feed Gases by Ion ChromatographyActive Standard ASTM D7550 | Developed by Subcommittee: D03.14 Book of Standards Volume: 05.06 ASTM D7550Significance and Use Low operating temperature fuel cells such as proton exchange membrane (PEM) fuel cells require high purity hydrogen for maximum material performance and lifetime. Analysis to part-per-billion (ppb) concentration of individual cation contaminants such as potassium, sodium and ammonium in hydrogen and related fuel cell supply gases is necessary for assuring a feed gas of sufficient purity to satisfy fuel cell system needs. More specifically, cations such as ammonium causes irreversible performance degradation of proton exchange membranes used in low temperature fuel cells by reacting with protons in the membrane to form ammonium ions. Although not intended for application to gases other than hydrogen and related fuel cell supply gases, techniques within this test method can be applied to other gaseous samples requiring cation analysis. 1. Scope 1.1 This test method describes a procedure for the determination of cations in hydrogen and other fuel cell feed gases. It has been successfully applied to other types of gaseous samples including air, engine exhaust, and landfill samples. An ion chromatograph/conductivity detector (IC/CD) system is used to determine cations. Sensitivity from low part per billion (ppb, ? g/l, ? g/kg) up to part per million (ppm, mg/l, mg/kg) concentration are achievable dependant on the amount of hydrogen or other fuel cell gas sampled. This test method can be applied to other gaseous samples requiring analysis of trace constituents provided an assessment of potential interferences has been accomplished. 1.2 The values stated in inch-pound units are to be regarded as standard. No other units of measurement are included in this standard. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
ASTM Standards D1193 Specification for Reagent Water Keywords ammonia; calcium; cations; fuel cells; gaseous fuels; hydrogen; ion chromatography; magnesium; PEM; potassium; proton exchange membrane; sampling; sodium; ICS Code ICS Number Code 27.070 (Fuel cells); 71.040.50 (Physicochemical methods of analysis) DOI: 10.1520/D7550-09 ASTM International is a member of CrossRef. ASTM D7550This book also exists in the following packages...Subscription InformationMADCAD.com ASTM Standards subscriptions are annual and access is unlimited concurrency based (number of people that can access the subscription at any given time) from single office location. For pricing on multiple office location ASTM Standards Subscriptions, please contact us at info@madcad.com or +1 800.798.9296.
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About ASTMASTM International, formerly known as the American Society for Testing and Materials (ASTM), is a globally recognized leader in the development and delivery of international voluntary consensus standards. Today, some 12,000 ASTM standards are used around the world to improve product quality, enhance safety, facilitate market access and trade, and build consumer confidence. ASTM’s leadership in international standards development is driven by the contributions of its members: more than 30,000 of the world’s top technical experts and business professionals representing 150 countries. Working in an open and transparent process and using ASTM’s advanced electronic infrastructure, ASTM members deliver the test methods, specifications, guides, and practices that support industries and governments worldwide. |
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